Information card for entry 7014973

Structure parameters

• Formula: C81.75 H80 Cl3.5 F12 N8 O4.25 Os2 P4
• Calculated formula: C81.75 H79.5 Cl3.5 F12 N8 O4.25 Os2 P4
• Title of publication: Binuclear (salen)osmium phosphinidine and phosphiniminato complexes.
• Authors of publication: Chen, Gui; Man, Wai-Lun; Yiu, Shek-Man; Wong, Tsz-Wing; Szeto, Lap; Wong, Wing-Tak; Lau, Tai-Chu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 9
• Pages of publication: 1938 - 1944
• a: 21.63349 ± 0.00015 Å
• b: 23.90315 ± 0.00017 Å
• c: 15.8906 ± 0.00013 Å
• α: 90°
• β: 90.6675 ± 0.0008°
• γ: 90°
• Cell volume: 8216.61 ± 0.11 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0861
• Weighted residual factors for all reflections included in the refinement: 0.0889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No