Crystallography Open Database

Information card for entry 7014974

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Structure parameters

Formula	C73 H75.5 F12 N8.5 O6 Os2 P4
Calculated formula	C73 H75.5 F12 N8.5 O6 Os2 P4
Title of publication	Binuclear (salen)osmium phosphinidine and phosphiniminato complexes.
Authors of publication	Chen, Gui; Man, Wai-Lun; Yiu, Shek-Man; Wong, Tsz-Wing; Szeto, Lap; Wong, Wing-Tak; Lau, Tai-Chu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	9
Pages of publication	1938 - 1944
a	19.3433 ± 0.0004 Å
b	16.2405 ± 0.0003 Å
c	25.737 ± 0.0005 Å
α	90°
β	105.477 ± 0.002°
γ	90°
Cell volume	7792 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0353
Weighted residual factors for significantly intense reflections	0.0648
Weighted residual factors for all reflections included in the refinement	0.0696
Goodness-of-fit parameter for all reflections included in the refinement	0.97
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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