Crystallography Open Database

Information card for entry 7015105

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Coordinates	7015105.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H60 Li2 N6 O2 Si2
Calculated formula	C38 H60 Li2 N6 O2 Si2
Title of publication	A bulky silyl shift-directed synthesis of a silyl-linked amidinate-amidine and its Zr(IV) complex.
Authors of publication	Tong, Hong-Bo; Li, Min; Bai, Sheng-Di; Yuan, Shi-Fang; Chao, Jian-Bin; Huang, Shuping; Liu, Dian-Sheng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	16
Pages of publication	4236 - 4241
a	11.089 ± 0.003 Å
b	12.471 ± 0.003 Å
c	17.197 ± 0.004 Å
α	81.586 ± 0.004°
β	75.624 ± 0.004°
γ	67.478 ± 0.004°
Cell volume	2124.5 ± 0.9 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1344
Residual factor for significantly intense reflections	0.0754
Weighted residual factors for significantly intense reflections	0.1268
Weighted residual factors for all reflections included in the refinement	0.1462
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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