Information card for entry 7015106

Structure parameters

• Formula: C58 H60 Li2 N10 Si2
• Calculated formula: C58 H60 Li2 N10 Si2
• SMILES: [Li]123[N](c4ccccc4)=C(c4ccccc4)N1[Si@](C)([N]1(C)C)NC(c4ccccc4)=[N](c4ccccc4)[Li]14[N](c1ccccc1)=C(c1ccccc1)N4[Si@@](C)([N]2(C)C)NC(c1ccccc1)=[N]3c1ccccc1
• Title of publication: A bulky silyl shift-directed synthesis of a silyl-linked amidinate-amidine and its Zr(IV) complex.
• Authors of publication: Tong, Hong-Bo; Li, Min; Bai, Sheng-Di; Yuan, Shi-Fang; Chao, Jian-Bin; Huang, Shuping; Liu, Dian-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 16
• Pages of publication: 4236 - 4241
• a: 10.66 ± 0.004 Å
• b: 11.667 ± 0.006 Å
• c: 12.924 ± 0.007 Å
• α: 115.39 ± 0.04°
• β: 97.71 ± 0.03°
• γ: 105.45 ± 0.04°
• Cell volume: 1341.5 ± 1.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1624
• Weighted residual factors for all reflections included in the refinement: 0.1697
• Goodness-of-fit parameter for all reflections included in the refinement: 1.181
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No