Information card for entry 7015138

Structure parameters

• Formula: C47 H89 Cl Li Lu N4 O3 Si4
• Calculated formula: C47 H65 Cl Li Lu N4 O3 Si4
• Title of publication: Rare earth metal bis(amide) complexes bearing amidinate ancillary ligands: synthesis, characterization, and performance as catalyst precursors for cis-1,4 selective polymerization of isoprene.
• Authors of publication: Luo, Yunjie; Fan, Shimin; Yang, Jianping; Fang, Jianghua; Xu, Ping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 12
• Pages of publication: 3053 - 3059
• a: 12.3218 ± 0.0012 Å
• b: 13.9301 ± 0.0013 Å
• c: 18.273 ± 0.002 Å
• α: 77.021 ± 0.008°
• β: 81.07 ± 0.008°
• γ: 71.718 ± 0.007°
• Cell volume: 2889.8 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0721
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.1367
• Weighted residual factors for all reflections included in the refinement: 0.149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No