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Information card for entry 7015690
Preview
Coordinates | 7015690.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H43 F Ni P2 |
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Calculated formula | C24 H43 F Ni P2 |
SMILES | c12c3cccc2C[P]([Ni]1([P](C3)(C(C)(C)C)C(C)(C)C)F)(C(C)(C)C)C(C)(C)C |
Title of publication | Nickel(II) hydride and fluoride pincer complexes and their reactivity with Lewis acids BX3·L (X = H, L = thf; X = F, L = Et2O). |
Authors of publication | Rossin, Andrea; Peruzzini, Maurizio; Zanobini, Fabrizio |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 17 |
Pages of publication | 4447 - 4452 |
a | 16.044 ± 0.007 Å |
b | 16.044 ± 0.008 Å |
c | 19.529 ± 0.01 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5027 ± 4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 110 |
Hermann-Mauguin space group symbol | I 41 c d |
Hall space group symbol | I 4bw -2c |
Residual factor for all reflections | 0.0595 |
Residual factor for significantly intense reflections | 0.0304 |
Weighted residual factors for significantly intense reflections | 0.0648 |
Weighted residual factors for all reflections included in the refinement | 0.0702 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.86 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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