Information card for entry 7016049

Structure parameters

• Formula: C47 H117 Ge9 Li Mo O6 Si12
• Calculated formula: C47 H117 Ge9 Li Mo O6 Si12
• Title of publication: [Si(SiMe(3))(3)](3)Ge(9)M(CO)(3)(-) (M = Cr, Mo, W): Coordination Chemistry with metalloid Clusters.
• Authors of publication: Henke, Florian; Schenk, Christian; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 25
• Pages of publication: 6704 - 6710
• a: 15.7684 ± 0.0008 Å
• b: 16.7824 ± 0.001 Å
• c: 32.886 ± 0.002 Å
• α: 90°
• β: 90.823 ± 0.008°
• γ: 90°
• Cell volume: 8701.8 ± 0.9 ų
• Cell temperature: 199 ± 2 K
• Ambient diffraction temperature: 199 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0784
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 0.866
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No