Information card for entry 7016050

Structure parameters

• Formula: C44.5 H119 Ge9 Li N4 O3 Si12 W
• Calculated formula: C44.5 H119 Ge9 Li N4 O3 Si12 W
• Title of publication: [Si(SiMe(3))(3)](3)Ge(9)M(CO)(3)(-) (M = Cr, Mo, W): Coordination Chemistry with metalloid Clusters.
• Authors of publication: Henke, Florian; Schenk, Christian; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 25
• Pages of publication: 6704 - 6710
• a: 25.736 ± 0.004 Å
• b: 25.736 ± 0.004 Å
• c: 26.755 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 17721 ± 5 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149 ± 2 K
• Number of distinct elements: 8
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0854
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections included in the refinement: 0.0776
• Goodness-of-fit parameter for all reflections included in the refinement: 0.906
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No