Information card for entry 7016187

Structure parameters

• Formula: C66 H83 I N7 O2 Si Sm3
• Calculated formula: C66 H83 I N7 O2 Si Sm3
• Title of publication: Cubic and doubly-fused cubic samarium clusters from Sm(ii)-mediated reduction of organic azides and azobenzenes.
• Authors of publication: Pan, Cheng-Ling; Chen, Wan; Su, Shengqun; Pan, Yu-Song; Wang, Jing
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 31
• Pages of publication: 7941 - 7945
• a: 12.7941 ± 0.001 Å
• b: 15.055 ± 0.0012 Å
• c: 20.126 ± 0.002 Å
• α: 109.655 ± 0.002°
• β: 94.921 ± 0.002°
• γ: 108.089 ± 0.001°
• Cell volume: 3391 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0508
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1654
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No