Zinc complexes of Ttz(R,Me) with O and S donors reveal differences between Tp and Ttz ligands: acid stability and binding to H or an additional metal (Ttz(R,Me) = tris(3-R-5-methyl-1,2,4-triazolyl)borate; R = Ph, tBu).
Authors of publication
Kumar, Mukesh; Papish, Elizabeth T.; Zeller, Matthias; Hunter, Allen D.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
29
Pages of publication
7517 - 7533
a
16.6709 ± 0.0014 Å
b
14.625 ± 0.0012 Å
c
18.4633 ± 0.0014 Å
α
90°
β
115.455 ± 0.002°
γ
90°
Cell volume
4064.6 ± 0.6 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0577
Residual factor for significantly intense reflections
0.0424
Weighted residual factors for significantly intense reflections
0.1156
Weighted residual factors for all reflections included in the refinement
0.1252
Goodness-of-fit parameter for all reflections included in the refinement
