Zinc complexes of Ttz(R,Me) with O and S donors reveal differences between Tp and Ttz ligands: acid stability and binding to H or an additional metal (Ttz(R,Me) = tris(3-R-5-methyl-1,2,4-triazolyl)borate; R = Ph, tBu).
Authors of publication
Kumar, Mukesh; Papish, Elizabeth T.; Zeller, Matthias; Hunter, Allen D.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
29
Pages of publication
7517 - 7533
a
17.1768 ± 0.0009 Å
b
11.6552 ± 0.0007 Å
c
16.1882 ± 0.0009 Å
α
90°
β
115.862 ± 0.001°
γ
90°
Cell volume
2916.3 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0411
Residual factor for significantly intense reflections
0.0342
Weighted residual factors for significantly intense reflections
0.0883
Weighted residual factors for all reflections included in the refinement
0.0931
Goodness-of-fit parameter for all reflections included in the refinement
