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Information card for entry 7016360
Preview
Coordinates | 7016360.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H39 F O11 P2 Sn W |
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Calculated formula | C27 H39 F O11 P2 Sn W |
SMILES | [W]([Sn]12(F)[O]=P(OC(C)C)(OC(C)C)c3c2c(P(=[O]1)(OC(C)C)OC(C)C)cc(c3)C(C)(C)C)(C#[O])(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | Intramolecularly coordinated heteroleptic organostannylene tungsten pentacarbonyl complexes 4-tBu-2,6-[P(O)(OiPr)(2)](2)C(6)H(2)Sn(X)W(CO)(5) (X = Cl, F, PPh(2), PPh(2)[W(CO)(5)]). Syntheses and reactivity. |
Authors of publication | Wagner, Michael; Dorogov, Konstantin; Schürmann, Markus; Jurkschat, Klaus |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 35 |
Pages of publication | 8839 - 8848 |
a | 10.6089 ± 0.0003 Å |
b | 11.7686 ± 0.0005 Å |
c | 15.4337 ± 0.0006 Å |
α | 78.061 ± 0.003° |
β | 72.319 ± 0.003° |
γ | 79.707 ± 0.003° |
Cell volume | 1782.26 ± 0.12 Å3 |
Cell temperature | 173 ± 1 K |
Ambient diffraction temperature | 173 ± 1 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0436 |
Residual factor for significantly intense reflections | 0.0363 |
Weighted residual factors for significantly intense reflections | 0.0903 |
Weighted residual factors for all reflections included in the refinement | 0.0919 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.988 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7016360.html
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Users of the data should acknowledge the original authors of the
structural data.