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Information card for entry 7016389
Preview
Coordinates | 7016389.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H64 Cl2 N O4 P Pd Si2 |
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Calculated formula | C46 H64 Cl2 N O4 P Pd Si2 |
Title of publication | Chiral palladacycles based on resorcinol monophosphite ligands: the role of the meta-hydroxyl in ligand C-H activation and catalysis. |
Authors of publication | Bedford, Robin B.; Chang, Yu-Ning; Haddow, Mairi F.; McMullin, Claire L. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 35 |
Pages of publication | 9042 - 9050 |
a | 27.163 ± 0.0004 Å |
b | 14.38 ± 0.0002 Å |
c | 14.1182 ± 0.0002 Å |
α | 90° |
β | 105.286 ± 0.001° |
γ | 90° |
Cell volume | 5319.53 ± 0.13 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.037 |
Residual factor for significantly intense reflections | 0.0321 |
Weighted residual factors for significantly intense reflections | 0.0725 |
Weighted residual factors for all reflections included in the refinement | 0.0745 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7016389.html
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