Information card for entry 7016390

Structure parameters

• Formula: C56.5 H56 Cl N3 P3 Rh
• Calculated formula: C56.5 H56 Cl N3 P3 Rh
• Title of publication: Pincer ligands with an all-phosphorus donor set: subtle differences between rhodium and palladium.
• Authors of publication: Bauer, Richard C.; Gloaguen, Yann; Lutz, Martin; Reek, Joost N. H.; de Bruin, Bas; van der Vlugt, Jarl Ivar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 35
• Pages of publication: 8822 - 8829
• a: 11.483 ± 0.0006 Å
• b: 12.4619 ± 0.0004 Å
• c: 18.65 ± 0.0006 Å
• α: 90.887 ± 0.002°
• β: 99.603 ± 0.002°
• γ: 109.56 ± 0.002°
• Cell volume: 2472.24 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0298
• Residual factor for significantly intense reflections: 0.0255
• Weighted residual factors for significantly intense reflections: 0.0624
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No