Information card for entry 7016457

Structure parameters

• Formula: K4 O24 Te3 V6
• Calculated formula: K4 O24 Te3 V6
• Title of publication: Synthesis and structure of A(4)V(6)[Te(2)(4+)Te(6+)]O(24) (A = K, Rb)-two new quaternary mixed-valent tellurium oxides.
• Authors of publication: Zhu, Tianxiang; Qin, Jingui; Halasyamani, P. Shiv
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 34
• Pages of publication: 8527 - 8532
• a: 9.7075 ± 0.0006 Å
• b: 9.7075 ± 0.0006 Å
• c: 42.701 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3484.8 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0186
• Residual factor for significantly intense reflections: 0.0177
• Weighted residual factors for significantly intense reflections: 0.0432
• Weighted residual factors for all reflections included in the refinement: 0.0435
• Goodness-of-fit parameter for all reflections included in the refinement: 1.215
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No