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Information card for entry 7016750
Preview
Coordinates | 7016750.cif |
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Original paper (by DOI) | HTML |
Formula | C186 H183.7 F48 Fe4 N27 O21.35 P8 |
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Calculated formula | C186 H165 F48 Fe4 N27 O21.35 P8 |
Title of publication | New nickel(ii) and iron(ii) helicates and tetrahedra derived from expanded quaterpyridines. |
Authors of publication | Glasson, Christopher R. K.; Meehan, George V.; Motti, Cherie A.; Clegg, Jack K.; Turner, Peter; Jensen, Paul; Lindoy, Leonard F. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 40 |
Pages of publication | 10481 - 10490 |
a | 20.247 ± 0.0012 Å |
b | 20.79 ± 0.0012 Å |
c | 30.546 ± 0.0017 Å |
α | 82.126 ± 0.003° |
β | 76.935 ± 0.003° |
γ | 73.436 ± 0.003° |
Cell volume | 11969 ± 1.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1473 |
Residual factor for significantly intense reflections | 0.1192 |
Weighted residual factors for significantly intense reflections | 0.3016 |
Weighted residual factors for all reflections included in the refinement | 0.3245 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.384 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7016750.html
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