Information card for entry 7016751

Structure parameters

• Formula: C264 H279.75 F48 N30 Ni4 O35.325 P8
• Calculated formula: C264 H272 F48 N30 Ni4 O35.325 P8
• Title of publication: New nickel(ii) and iron(ii) helicates and tetrahedra derived from expanded quaterpyridines.
• Authors of publication: Glasson, Christopher R. K.; Meehan, George V.; Motti, Cherie A.; Clegg, Jack K.; Turner, Peter; Jensen, Paul; Lindoy, Leonard F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10481 - 10490
• a: 21.1588 ± 0.0012 Å
• b: 24.2022 ± 0.0014 Å
• c: 37.7344 ± 0.0022 Å
• α: 78.498 ± 0.004°
• β: 79.573 ± 0.004°
• γ: 76.78 ± 0.003°
• Cell volume: 18247 ± 1.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1719
• Residual factor for significantly intense reflections: 0.1123
• Weighted residual factors for significantly intense reflections: 0.2757
• Weighted residual factors for all reflections included in the refinement: 0.3001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.173
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No