Information card for entry 7017463

Structure parameters

• Formula: C26 H46 Cl N3 Si2
• Calculated formula: C26 H46 Cl N3 Si2
• SMILES: [Si](Cl)(N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)=C1N(C(C)=C(N1C(C)C)C)C(C)C
• Title of publication: Silylation of N-heterocyclic carbene with aminochlorosilane and -disilane: dehydrohalogenation vs. Si-Si bond cleavage.
• Authors of publication: Cui, Haiyan; Cui, Chunming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11937 - 11940
• a: 10.3126 ± 0.0017 Å
• b: 17.824 ± 0.003 Å
• c: 15.921 ± 0.003 Å
• α: 90°
• β: 102.561 ± 0.002°
• γ: 90°
• Cell volume: 2856.4 ± 0.9 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0627
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No