Information card for entry 7017464

Structure parameters

• Formula: C26 H47 Cl N3 Si2
• Calculated formula: C26 H46 Cl N3 Si2
• SMILES: Cl[SiH](N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)C1N([C]N(C=1)C(C)(C)C)C(C)(C)C
• Title of publication: Silylation of N-heterocyclic carbene with aminochlorosilane and -disilane: dehydrohalogenation vs. Si-Si bond cleavage.
• Authors of publication: Cui, Haiyan; Cui, Chunming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11937 - 11940
• a: 10.129 ± 0.002 Å
• b: 17.177 ± 0.003 Å
• c: 34.277 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5964 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0662
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1317
• Weighted residual factors for all reflections included in the refinement: 0.1363
• Goodness-of-fit parameter for all reflections included in the refinement: 1.144
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No