Information card for entry 7017941

Structure parameters

• Formula: C12 H28 Cl Co N4 O6
• Calculated formula: C12 H28 Cl Co N4 O6
• Title of publication: High diastereoselectivity in borohydride reductions of coordinated imines.
• Authors of publication: Wilson-Coutts, Sarah M; Browne, Julian M. W.; Marsh, Liesl C.; Polson, Matthew I. J.; Hartshorn, Richard M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 1591 - 1596
• a: 7.5702 ± 0.0012 Å
• b: 21.16 ± 0.003 Å
• c: 12.3205 ± 0.0019 Å
• α: 90°
• β: 96.93 ± 0.008°
• γ: 90°
• Cell volume: 1959.1 ± 0.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1688
• Residual factor for significantly intense reflections: 0.1291
• Weighted residual factors for significantly intense reflections: 0.3195
• Weighted residual factors for all reflections included in the refinement: 0.3428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No