Information card for entry 7017942

Structure parameters

• Formula: C35 H52 N4 O4 Si
• Calculated formula: C35 H52 N4 O4 Si
• Title of publication: Double N-H bond activation of N,N'-bis-substituted hydrazines with stable N-heterocyclic silylene.
• Authors of publication: Azhakar, Ramachandran; Ghadwal, Rajendra S.; Roesky, Herbert W.; Hey, Jakob; Stalke, Dietmar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 1529 - 1533
• a: 13.2681 ± 0.0014 Å
• b: 12.0341 ± 0.0012 Å
• c: 21.837 ± 0.002 Å
• α: 90°
• β: 94.78 ± 0.005°
• γ: 90°
• Cell volume: 3474.6 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.06
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.1119
• Weighted residual factors for all reflections included in the refinement: 0.1181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No