Information card for entry 7017944

Structure parameters

• Formula: C33 H48 N4 O2 Si
• Calculated formula: C33 H48 N4 O2 Si
• SMILES: [SiH]12(OC(=NN2C(=O)C)C)N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C
• Title of publication: Double N-H bond activation of N,N'-bis-substituted hydrazines with stable N-heterocyclic silylene.
• Authors of publication: Azhakar, Ramachandran; Ghadwal, Rajendra S.; Roesky, Herbert W.; Hey, Jakob; Stalke, Dietmar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 1529 - 1533
• a: 13.816 ± 0.002 Å
• b: 14.387 ± 0.002 Å
• c: 15.751 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3130.8 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0873
• Weighted residual factors for all reflections included in the refinement: 0.0914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No