Information card for entry 7017943

Structure parameters

• Formula: C39.12 H55.24 N4 O Si
• Calculated formula: C39.12 H55.24 N4 O Si
• Title of publication: Double N-H bond activation of N,N'-bis-substituted hydrazines with stable N-heterocyclic silylene.
• Authors of publication: Azhakar, Ramachandran; Ghadwal, Rajendra S.; Roesky, Herbert W.; Hey, Jakob; Stalke, Dietmar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 1529 - 1533
• a: 11.4828 ± 0.0008 Å
• b: 12.0258 ± 0.0009 Å
• c: 26.1609 ± 0.0019 Å
• α: 90°
• β: 94.746 ± 0.002°
• γ: 90°
• Cell volume: 3600.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No