Information card for entry 7019156

Structure parameters

• Formula: C16 H39 Cl2 N3 Ni P2
• Calculated formula: C16 H39 Cl2 N3 Ni P2
• SMILES: [Ni]12(Cl)[P](NCC[NH]2CCN[P]1(C(C)C)C(C)C)(C(C)C)C(C)C.[Cl-]
• Title of publication: Ni(ii), Pd(ii) and Pt(ii) complexes of PNP and PSP tridentate amino-phosphine ligands.
• Authors of publication: Sgro, Michael J.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 22
• Pages of publication: 6791 - 6802
• a: 15.6535 ± 0.0009 Å
• b: 18.4051 ± 0.001 Å
• c: 27.97 ± 0.002 Å
• α: 104.784 ± 0.003°
• β: 97.91 ± 0.003°
• γ: 109.773 ± 0.002°
• Cell volume: 7106.6 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0658
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0998
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No