Information card for entry 7019157

Structure parameters

• Formula: C16 H39 Cl2 N3 P2 Pd
• Calculated formula: C16 H39 Cl2 N3 P2 Pd
• SMILES: [Pd]12(Cl)[P](NCC[NH]2CCN[P]1(C(C)C)C(C)C)(C(C)C)C(C)C.[Cl-]
• Title of publication: Ni(ii), Pd(ii) and Pt(ii) complexes of PNP and PSP tridentate amino-phosphine ligands.
• Authors of publication: Sgro, Michael J.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 22
• Pages of publication: 6791 - 6802
• a: 23.205 ± 0.006 Å
• b: 10.981 ± 0.002 Å
• c: 8.9992 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2293.1 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0745
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No