Information card for entry 7019243

Structure parameters

• Formula: C54 H66 Er N3 P2 Si2
• Calculated formula: C54 H66 Er N3 P2 Si2
• Title of publication: Thermally stable rare earth dialkyl complexes supported by a novel bis(phosphinimine)pyrrole ligand.
• Authors of publication: Johnson, Kevin R. D.; Hannon, Matt A.; Ritch, Jamie S.; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 26
• Pages of publication: 7873 - 7875
• a: 9.729 ± 0.005 Å
• b: 12.188 ± 0.006 Å
• c: 24.287 ± 0.011 Å
• α: 84.796 ± 0.005°
• β: 78.92 ± 0.005°
• γ: 69.55 ± 0.005°
• Cell volume: 2647 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0818
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No