Crystallography Open Database

Information card for entry 7019244

7019243 << 7019244 >> 7019245

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Coordinates	7019244.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H66 Lu N3 P2 Si2
Calculated formula	C54 H66 Lu N3 P2 Si2
Title of publication	Thermally stable rare earth dialkyl complexes supported by a novel bis(phosphinimine)pyrrole ligand.
Authors of publication	Johnson, Kevin R. D.; Hannon, Matt A.; Ritch, Jamie S.; Hayes, Paul G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	26
Pages of publication	7873 - 7875
a	9.7163 ± 0.0006 Å
b	12.1266 ± 0.0007 Å
c	24.2569 ± 0.0014 Å
α	84.953 ± 0.001°
β	78.922 ± 0.001°
γ	69.464 ± 0.001°
Cell volume	2625.9 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0346
Residual factor for significantly intense reflections	0.03
Weighted residual factors for significantly intense reflections	0.0721
Weighted residual factors for all reflections included in the refinement	0.0746
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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