Information card for entry 7019312

Structure parameters

• Formula: C36.2 H25 Cl2 F3 N3 O3.55 S Sb
• Calculated formula: C36.2 H25 Cl2 F3 N3 O3.55 S Sb
• Title of publication: Chemistry of the heavy group 15 elements with the pyridyl tethered 1,2-bis(imino)acenaphthene "clamshell" ligand.
• Authors of publication: Brazeau, Allison L.; Jones, Nathan D.; Ragogna, Paul J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 26
• Pages of publication: 7890 - 7896
• a: 12.5743 ± 0.001 Å
• b: 20.9295 ± 0.0017 Å
• c: 14.73 ± 0.0011 Å
• α: 90°
• β: 93.609 ± 0.002°
• γ: 90°
• Cell volume: 3868.9 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1091
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.1584
• Weighted residual factors for all reflections included in the refinement: 0.1905
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No