Information card for entry 7019313

Structure parameters

• Formula: C36 H29 Bi Cl6 F3 N3 O3 S
• Calculated formula: C36 H29 Bi Cl6 F3 N3 O3 S
• Title of publication: Chemistry of the heavy group 15 elements with the pyridyl tethered 1,2-bis(imino)acenaphthene "clamshell" ligand.
• Authors of publication: Brazeau, Allison L.; Jones, Nathan D.; Ragogna, Paul J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 26
• Pages of publication: 7890 - 7896
• a: 42.4663 ± 0.0017 Å
• b: 9.7165 ± 0.0005 Å
• c: 20.6524 ± 0.0008 Å
• α: 90°
• β: 110.538 ± 0.002°
• γ: 90°
• Cell volume: 7980 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.074
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0765
• Weighted residual factors for all reflections included in the refinement: 0.0865
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No