Information card for entry 7019739

Structure parameters

• Formula: C108 H106 Br1.4 Cl14.46 N10 O29 Sb12 Sr0.14 Zn4.86
• Calculated formula: C108 H96 Br1.4 Cl14.46 N10 O29 Sb12 Sr0.14 Zn4.86
• Title of publication: Isopolyoxometalates derived from arylstibonic acids with "reverse-Keggin ion" structures based on [M(RSb)(12)O(28)] cores, M = Co(ii) or Zn(ii).
• Authors of publication: Nicholson, Brian K.; Clark, Christopher J.; Telfer, Shane G.; Groutso, Tania
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 33
• Pages of publication: 9964 - 9970
• a: 15.293 ± 0.0002 Å
• b: 25.0465 ± 0.0004 Å
• c: 19.1113 ± 0.0003 Å
• α: 90°
• β: 92.597 ± 0.001°
• γ: 90°
• Cell volume: 7312.8 ± 0.19 ų
• Cell temperature: 89 ± 2 K
• Ambient diffraction temperature: 89 ± 2 K
• Number of distinct elements: 9
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No