Information card for entry 7019740

Structure parameters

• Formula: C72 H116 Cl14 Co5 O62 Sb12
• Calculated formula: C72 H48 Cl13.995 Co5 O62 Sb12
• Title of publication: Isopolyoxometalates derived from arylstibonic acids with "reverse-Keggin ion" structures based on [M(RSb)(12)O(28)] cores, M = Co(ii) or Zn(ii).
• Authors of publication: Nicholson, Brian K.; Clark, Christopher J.; Telfer, Shane G.; Groutso, Tania
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 33
• Pages of publication: 9964 - 9970
• a: 23.7522 ± 0.0003 Å
• b: 23.7522 ± 0.0003 Å
• c: 44.6195 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 21800.3 ± 0.8 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 155
• Hermann-Mauguin space group symbol: R 3 2 :H
• Hall space group symbol: R 3 2"
• Residual factor for all reflections: 0.0314
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No