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Information card for entry 7020673
Preview
Coordinates | 7020673.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H31 F8.38 N10 O4.42 P1.4 Re1.61 |
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Calculated formula | C22 H31 F8.37 N10 O4.42 P1.395 Re1.605 |
Title of publication | Trans [O=Re(V)-OH] core stabilised by chelating N-heterocyclic dicarbene ligands. |
Authors of publication | Lum, Regina; Zhang, Hu; Zhang, Wenhua; Bai, Shi-Qiang; Zhao, Jin; Hor, T. S. Andy |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2013 |
Journal volume | 42 |
Journal issue | 4 |
Pages of publication | 871 - 873 |
a | 8.333 ± 0.0005 Å |
b | 9.7967 ± 0.0006 Å |
c | 11.514 ± 0.0007 Å |
α | 112.133 ± 0.001° |
β | 97.526 ± 0.001° |
γ | 101.004 ± 0.001° |
Cell volume | 833.14 ± 0.09 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0407 |
Residual factor for significantly intense reflections | 0.0386 |
Weighted residual factors for significantly intense reflections | 0.0915 |
Weighted residual factors for all reflections included in the refinement | 0.0925 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.243 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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