Crystallography Open Database

Information card for entry 7020674

7020673 << 7020674 >> 7020675

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Coordinates	7020674.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H41 F8.44 N8 O4.37 P1.41 Re1.59
Calculated formula	C26 H41 F8.442 N8 O4.372 P1.407 Re1.593
Title of publication	Trans [O=Re(V)-OH] core stabilised by chelating N-heterocyclic dicarbene ligands.
Authors of publication	Lum, Regina; Zhang, Hu; Zhang, Wenhua; Bai, Shi-Qiang; Zhao, Jin; Hor, T. S. Andy
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	4
Pages of publication	871 - 873
a	9.0425 ± 0.001 Å
b	17.8358 ± 0.0019 Å
c	11.7838 ± 0.0013 Å
α	90°
β	110.328 ± 0.003°
γ	90°
Cell volume	1782.1 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.045
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.1039
Weighted residual factors for all reflections included in the refinement	0.1042
Goodness-of-fit parameter for all reflections included in the refinement	1.27
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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