Information card for entry 7021610

Structure parameters

• Formula: C20 H18 N3 O3 V
• Calculated formula: C20 H18 N3 O3 V
• SMILES: [V]123(Oc4c([N]3(c3c(O1)cccc3)c1c(O2)cccc1)cccc4)=NN(C)C
• Title of publication: Synthesis of vanadium(v) hydrazido complexes with tris(2-hydroxyphenyl)amine ligands.
• Authors of publication: Moriuchi, Toshiyuki; Ikeuchi, Kousuke; Hirao, Toshikazu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 33
• Pages of publication: 11824 - 11830
• a: 16.2235 ± 0.0005 Å
• b: 11.824 ± 0.0003 Å
• c: 18.6632 ± 0.0005 Å
• α: 90°
• β: 96.464 ± 0.001°
• γ: 90°
• Cell volume: 3557.34 ± 0.17 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0673
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No