Information card for entry 7021611

Structure parameters

• Formula: C42 H42 F2 N8 O6 V2
• Calculated formula: C42 H42 F2 N8 O6 V2
• Title of publication: Synthesis of vanadium(v) hydrazido complexes with tris(2-hydroxyphenyl)amine ligands.
• Authors of publication: Moriuchi, Toshiyuki; Ikeuchi, Kousuke; Hirao, Toshikazu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 33
• Pages of publication: 11824 - 11830
• a: 9.3304 ± 0.0011 Å
• b: 18.403 ± 0.002 Å
• c: 12.1985 ± 0.0014 Å
• α: 90°
• β: 102.631 ± 0.003°
• γ: 90°
• Cell volume: 2043.9 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1353
• Residual factor for significantly intense reflections: 0.0742
• Weighted residual factors for significantly intense reflections: 0.1511
• Weighted residual factors for all reflections included in the refinement: 0.1803
• Goodness-of-fit parameter for all reflections included in the refinement: 0.97
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No