Information card for entry 7021655

Structure parameters

• Formula: C50.5 H58 B2 F24 P2
• Calculated formula: C50.5 H58 B2 F24 P2
• Title of publication: Bis(phosphine)boronium salts. Synthesis, structures and coordination chemistry.
• Authors of publication: Shuttleworth, Timothy A.; Huertos, Miguel A.; Pernik, Indrek; Young, Rowan D.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 12917 - 12925
• a: 15.974 ± 0.0001 Å
• b: 18.196 ± 0.0001 Å
• c: 20.965 ± 0.0002 Å
• α: 90°
• β: 111.804 ± 0.0003°
• γ: 90°
• Cell volume: 5657.8 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0561
• Weighted residual factors for significantly intense reflections: 0.1348
• Weighted residual factors for all reflections included in the refinement: 0.1502
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No