Information card for entry 7021656

Structure parameters

• Formula: C99 H71 B2 Cl2 F24 P4 Rh
• Calculated formula: C99 H71 B2 Cl2 F24 P4 Rh
• Title of publication: Bis(phosphine)boronium salts. Synthesis, structures and coordination chemistry.
• Authors of publication: Shuttleworth, Timothy A.; Huertos, Miguel A.; Pernik, Indrek; Young, Rowan D.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 12917 - 12925
• a: 12.9019 ± 0.0003 Å
• b: 17.27 ± 0.0004 Å
• c: 21.5728 ± 0.0005 Å
• α: 99.512 ± 0.002°
• β: 91.448 ± 0.002°
• γ: 99.925 ± 0.002°
• Cell volume: 4662.57 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for significantly intense reflections: 0.1771
• Weighted residual factors for all reflections included in the refinement: 0.1848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No