Reactivity differences between 2,4- and 2,5-disubstituted zirconacyclopentadienes: a highly selective and general approach to 2,4-disubstituted phospholes.
Authors of publication
Bousrez, Guillaume; Jaroschik, Florian; Martinez, Agathe; Harakat, Dominique; Nicolas, Emmanuel; Le Goff, Xavier F.; Szymoniak, Jan
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
30
Pages of publication
10997 - 11004
a
5.884 ± 0.001 Å
b
8.898 ± 0.001 Å
c
30.968 ± 0.001 Å
α
90°
β
96.658 ± 0.002°
γ
90°
Cell volume
1610.4 ± 0.3 Å3
Cell temperature
150 ± 0.1 K
Ambient diffraction temperature
150 ± 0.1 K
Number of distinct elements
3
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0522
Residual factor for significantly intense reflections
0.0462
Weighted residual factors for significantly intense reflections
0.1149
Weighted residual factors for all reflections included in the refinement
0.1199
Goodness-of-fit parameter for all reflections included in the refinement
