Reactivity differences between 2,4- and 2,5-disubstituted zirconacyclopentadienes: a highly selective and general approach to 2,4-disubstituted phospholes.
Authors of publication
Bousrez, Guillaume; Jaroschik, Florian; Martinez, Agathe; Harakat, Dominique; Nicolas, Emmanuel; Le Goff, Xavier F.; Szymoniak, Jan
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
30
Pages of publication
10997 - 11004
a
12.079 ± 0.001 Å
b
5.832 ± 0.001 Å
c
12.562 ± 0.001 Å
α
90°
β
115.528 ± 0.001°
γ
90°
Cell volume
798.54 ± 0.16 Å3
Cell temperature
150 ± 0.1 K
Ambient diffraction temperature
150 ± 0.1 K
Number of distinct elements
3
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0378
Residual factor for significantly intense reflections
0.0359
Weighted residual factors for significantly intense reflections
0.0788
Weighted residual factors for all reflections included in the refinement
0.0806
Goodness-of-fit parameter for all reflections included in the refinement
