Information card for entry 7023500

Structure parameters

• Formula: C40 H78 Bi2 N4 O4 Si4
• Calculated formula: C40 H78 Bi2 N4 O4 Si4
• Title of publication: Synthesis of metallasiloxanes of group 13-15 and their application in catalysis.
• Authors of publication: Li, Yan; Wang, Jinjin; Wu, Yile; Zhu, Hongping; Samuel, Prinson P.; Roesky, Herbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 37
• Pages of publication: 13715 - 13722
• a: 9.819 ± 0.002 Å
• b: 11.045 ± 0.003 Å
• c: 13.189 ± 0.003 Å
• α: 111.32 ± 0.02°
• β: 97.198 ± 0.019°
• γ: 101.63 ± 0.02°
• Cell volume: 1273.8 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1278
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1537
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No