Information card for entry 7023501

Structure parameters

• Formula: C64 H118 N4 O8 Sb2 Si8
• Calculated formula: C64 H118 N4 O8 Sb2 Si8
• SMILES: N(c1c(C(C)C)cccc1C(C)C)([Si@@](O[Sb]1O[Si](N(c2c(cccc2C(C)C)C(C)C)[Si](C)(C)C)(O[Sb](O[Si](N(c2c(cccc2C(C)C)C(C)C)[Si](C)(C)C)(O1)C)O[Si@@](N(c1c(cccc1C(C)C)C(C)C)[Si](C)(C)C)(O)C)C)(O)C)[Si](C)(C)C
• Title of publication: Synthesis of metallasiloxanes of group 13-15 and their application in catalysis.
• Authors of publication: Li, Yan; Wang, Jinjin; Wu, Yile; Zhu, Hongping; Samuel, Prinson P.; Roesky, Herbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 37
• Pages of publication: 13715 - 13722
• a: 9.7585 ± 0.0007 Å
• b: 14.3218 ± 0.0009 Å
• c: 14.4294 ± 0.0009 Å
• α: 82.922 ± 0.005°
• β: 86.529 ± 0.005°
• γ: 86.857 ± 0.005°
• Cell volume: 1995.3 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.0696
• Weighted residual factors for all reflections included in the refinement: 0.076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No