Information card for entry 7024276

Structure parameters

• Formula: C29 H41 Ge N5
• Calculated formula: C29 H41 Ge N5
• SMILES: [Ge]1(N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)N=N#N
• Title of publication: Reactivity of germanium(II) hydride with nitrous oxide, trimethylsilyl azide, ketones, and alkynes and the reaction of a methyl analogue with trimethylsilyl diazomethane.
• Authors of publication: Jana, Anukul; Roesky, Herbert W.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 132 - 138
• a: 16.697 ± 0.003 Å
• b: 17.006 ± 0.003 Å
• c: 17.763 ± 0.004 Å
• α: 101.17 ± 0.03°
• β: 116.15 ± 0.03°
• γ: 100.6 ± 0.03°
• Cell volume: 4229 ± 2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.09
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.1019
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No