Information card for entry 7024279

Structure parameters

• Formula: C37 H47 F3 Ge N2 O
• Calculated formula: C37 H47 F3 Ge N2 O
• SMILES: [Ge]1(OC(C(F)(F)F)c2ccccc2)N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C
• Title of publication: Reactivity of germanium(II) hydride with nitrous oxide, trimethylsilyl azide, ketones, and alkynes and the reaction of a methyl analogue with trimethylsilyl diazomethane.
• Authors of publication: Jana, Anukul; Roesky, Herbert W.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 132 - 138
• a: 10.833 ± 0.002 Å
• b: 11.879 ± 0.002 Å
• c: 14.5 ± 0.003 Å
• α: 79.54 ± 0.03°
• β: 83.1 ± 0.03°
• γ: 69.63 ± 0.03°
• Cell volume: 1716.9 ± 0.7 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0968
• Residual factor for significantly intense reflections: 0.0724
• Weighted residual factors for significantly intense reflections: 0.188
• Weighted residual factors for all reflections included in the refinement: 0.2109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No