Information card for entry 7024278

Structure parameters

• Formula: C37 H52 Ge N2 O4
• Calculated formula: C37 H52 Ge N2 O4
• SMILES: [Ge]1(N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)C(=C\C(=O)OCC)/C(=O)OCC
• Title of publication: Reactivity of germanium(II) hydride with nitrous oxide, trimethylsilyl azide, ketones, and alkynes and the reaction of a methyl analogue with trimethylsilyl diazomethane.
• Authors of publication: Jana, Anukul; Roesky, Herbert W.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 132 - 138
• a: 11.837 ± 0.002 Å
• b: 17.042 ± 0.003 Å
• c: 17.895 ± 0.004 Å
• α: 90°
• β: 103.69 ± 0.03°
• γ: 90°
• Cell volume: 3507.3 ± 1.2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0341
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No