Information card for entry 7024337

Structure parameters

• Formula: C41 H50 Cl Ge N2 P
• Calculated formula: C41 H50 Cl Ge N2 P
• SMILES: [Ge]1(Cl)[N](c2c(cccc2C(C)C)C(C)C)=C(CP(c2ccccc2)c2ccccc2)C=C(N1c1c(cccc1C(C)C)C(C)C)C
• Title of publication: Synthesis of phosphine substituted beta-diketiminate based isomeric Ge(II) complexes.
• Authors of publication: Reddy, N. Dastagiri; Jana, Anukul; Roesky, Herbert W.; Samuel, Prinson P.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 234 - 238
• a: 10.06 ± 0.002 Å
• b: 25.67 ± 0.005 Å
• c: 29.272 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7559 ± 3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.0861
• Weighted residual factors for all reflections included in the refinement: 0.0911
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No