Information card for entry 7024338

Structure parameters

• Formula: C41 H50 Cl Ge N2 P
• Calculated formula: C41 H50 Cl Ge N2 P
• SMILES: [Ge]1(Cl)[P](c2ccccc2)(c2ccccc2)C(=C(N1c1c(cccc1C(C)C)C(C)C)C)C(=N\c1c(cccc1C(C)C)C(C)C)\C
• Title of publication: Synthesis of phosphine substituted beta-diketiminate based isomeric Ge(II) complexes.
• Authors of publication: Reddy, N. Dastagiri; Jana, Anukul; Roesky, Herbert W.; Samuel, Prinson P.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 234 - 238
• a: 11.003 ± 0.002 Å
• b: 11.678 ± 0.002 Å
• c: 16.335 ± 0.003 Å
• α: 86.03 ± 0.03°
• β: 87.29 ± 0.03°
• γ: 67.4 ± 0.03°
• Cell volume: 1932.6 ± 0.7 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1199
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No