Information card for entry 7024802

Structure parameters

• Formula: C12 H28 O4 P2 Pb Se4
• Calculated formula: C12 H28 O4 P2 Pb Se4
• Title of publication: Synthesis and characterization of [Pb{Se2P(OiPr)2}2]n pseudo polymorphs: polymeric, single source precursor enabling preparation of shape-controlled lead selenide structures.
• Authors of publication: Chang, Wen-Shiang; Lin, Yi-Feng; Sarkar, Bijay; Chang, Yu-Min; Liu, Ling-Kang; Liu, C. W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 11
• Pages of publication: 2821 - 2830
• a: 24.636 ± 0.0011 Å
• b: 11.156 ± 0.0005 Å
• c: 8.6199 ± 0.0004 Å
• α: 90°
• β: 93.029 ± 0.001°
• γ: 90°
• Cell volume: 2365.78 ± 0.19 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0303
• Residual factor for significantly intense reflections: 0.0224
• Weighted residual factors for significantly intense reflections: 0.0574
• Weighted residual factors for all reflections included in the refinement: 0.068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.137
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No