Information card for entry 7024803

Structure parameters

• Formula: C30 H70 O8 P4 Pb2 Se8
• Calculated formula: C30 H70 O8 P4 Pb2 Se8
• SMILES: CCCCCC.[Pb]([Se]P(OC(C)C)(OC(C)C)=[Se])[Se]P(OC(C)C)(OC(C)C)=[Se]
• Title of publication: Synthesis and characterization of [Pb{Se2P(OiPr)2}2]n pseudo polymorphs: polymeric, single source precursor enabling preparation of shape-controlled lead selenide structures.
• Authors of publication: Chang, Wen-Shiang; Lin, Yi-Feng; Sarkar, Bijay; Chang, Yu-Min; Liu, Ling-Kang; Liu, C. W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 11
• Pages of publication: 2821 - 2830
• a: 9.5929 ± 0.0004 Å
• b: 10.7784 ± 0.0005 Å
• c: 13.7982 ± 0.0006 Å
• α: 81.033 ± 0.001°
• β: 83.862 ± 0.001°
• γ: 82.942 ± 0.001°
• Cell volume: 1392.95 ± 0.11 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0656
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No