Information card for entry 7024867

Structure parameters

• Formula: C18 H26 N O5 P S Si2 W
• Calculated formula: C18 H26 N O5 P S Si2 W
• Title of publication: Novel access to azaphosphiridine complexes and first applications using Brønsted acid-induced ring expansion reactions.
• Authors of publication: Fankel, Stefan; Helten, Holger; von Frantzius, Gerd; Schnakenburg, Gregor; Daniels, Jörg; Chu, Victoria; Müller, Christina; Streubel, Rainer
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 14
• Pages of publication: 3472 - 3481
• a: 9.3006 ± 0.0004 Å
• b: 9.8061 ± 0.0004 Å
• c: 15.3241 ± 0.0006 Å
• α: 72.925 ± 0.003°
• β: 75.155 ± 0.003°
• γ: 77.227 ± 0.003°
• Cell volume: 1275.21 ± 0.09 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0358
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No