Information card for entry 7025187

Structure parameters

• Formula: C48 H74 Al2 Cl4 N2 O6 P2 Si2
• Calculated formula: C48 H74 Al2 Cl4 N2 O6 P2 Si2
• Title of publication: Reactivity of Zn(II), Mg(II) and Al(III) chlorides with a phosphinimine ligand: new tetrameric inverse crown ether structures.
• Authors of publication: Valerio Cárdenas, Cintya; Muñoz Hernández, Miguel Angel; Grévy, Jean-Michel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6441 - 6448
• a: 9.3733 ± 0.0009 Å
• b: 11.8131 ± 0.0012 Å
• c: 14.4903 ± 0.0014 Å
• α: 114.008 ± 0.001°
• β: 91.232 ± 0.002°
• γ: 103.912 ± 0.002°
• Cell volume: 1409.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0525
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1333
• Weighted residual factors for all reflections included in the refinement: 0.139
• Goodness-of-fit parameter for all reflections included in the refinement: 0.8
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No